黄量教授论文集 1951-1999【2025|PDF|Epub|mobi|kindle电子书版本百度云盘下载】

黄量教授论文集 1951-1999PDF格式电子书版下载

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一．有机化学理论及化学反应的研究1

1.Many-membered carbon rings.Ⅳ.Synthesis of cyclononyne and cyclodecyne1

2.Many-membered carbon rings.Ⅵ.Unsaturated nine-membered cyclic hydrocarbons2

3.Many-membered carbon rings.Ⅶ.Cyclooctyne7

4.The hydrolysis of substitued ethyl p-biphenyl-carboxylates9

6.高效酰化催化剂——4-二甲氨基吡啶的合成19

7.异三尖杉酯碱的合成及异构体的分离22

8.S-及R-对甲苯亚磺酸I-薄荷醇酯的合成及两异构体的分离23

9.瑞氏（Reformasky）反应制备α-烷氧基-β-羟基羧酸酯26

10.A novel free radical rearrangement28

11.Solvent participation of Wittig olefination reaction in methanol30

12.Diels-Alder Reactions of 3-carboethoxy-and 3-Carbonitrile-2-Cyclohexen-1-one32

13.Intramolecular Induction of Asymmetric Darzen's Condensation of Aldehydes with Chiral α-Chloroacetates34

14.(+)-1S,2R,5S-8-β-萘基薄荷醇的合成36

二．抗肿瘤、抗病毒及防癌药物的研究42

1.抗癌药研究 Ⅰ.谷氨酰胺衍生物的合成42

2.抗病毒药物的研究Ⅲ.芳香α-酮醛的合成48

3.抗病毒药物的研究Ⅱ.乙酰苯衍生物的合成61

4.抗肿瘤药物的研究Ⅴ.谷氨酰胺衍生物的合成66

5.The synthesis and antitumor activity of kethoxal bis-thiosemicarbazone and its related compounds76

6.抗肿瘤及抗病毒药物的研究Ⅳ.α-酮醛与肼、羟胺及芳胺缩合化合物的合成87

7.抗肿瘤及抗病毒药物的研究Ⅴ.β-乙氧基-α-正丁酮醛双缩氨硫脲类似物的合成99

8.霉变食品中新亚硝胺：N-3-甲基丁基-N-1-甲基丙酮基亚硝胺105

9.A new N-nitroso compound,N-3- methylbutyl N-1- methylacetonyl-nitrosamine,in corn-bread inoculated with fungi112

10.农吉利抗癌有效成分的分离及其衍生物的合成120

11.抗肿瘤及抗病毒药物的研究Ⅵ.消旋β-邻苯二甲酰亚氨-α-正丁酮醛衍生物的合成126

12.防癌药物的研究——维生素甲酸衍生物的合成131

13.N-3-甲基丁基-N—1’-甲基丙酮基亚硝胺的合成140

14.24个新维甲酸衍生物对人食管癌细胞株克隆三（Eca109-C3）增殖的影响145

15.N，N-双（β-氯乙基）N'，N"-二（乙氧羰-[14C]甲基）-磷三酰胺（I）的合成151

16.抗白血病药物靛玉红的N1 取代物的合成154

17.二胺及其衍生物对体内小鼠S180鸟氨酸脱羧酶活性的影响159

18.抗白血病药物靛玉红以及靛蓝和异靛蓝衍生物的合成164

19.中药青黛中几种微量成分的研究.Ⅰ.吲哚并[2,1b]喹唑啉-6，12-二酮和青黛酮的分离、结构鉴定及合成170

20.三尖杉酯碱的半合成177

21.三尖杉酯碱的半合成178

22.半合成差向异构体三尖杉酯碱和表三尖杉酯碱的分离和鉴定180

23.新抗癌有效成分海南粗榧内酯（Hainanolide）结构的研究184

24.三尖杉酯碱的半合成189

25.Partial Synthesis of Harringtonine199

26.海南粗榧中的微量生物碱212

27.半合成差向异构体——三尖杉酯硷和表三尖杉酯硷的制备型高效液相色谱分离及鉴定217

28.几种三尖杉酯碱衍生物的合成219

29.脱氧三尖杉酯碱和高三尖杉酯碱的立体专一性合成223

30.异三尖杉酯碱的合成及其异构体的分离229

31.Study on the total synthesis of Hainanolide---construction of tricyclic intermediate(1)237

32.Study on the total synthesis of Hainanolide(Ⅱ)-An unexpected hydroperoxide containing tricyclic skeleton239

33.Studies on the total synthesis of Hainanolide(Ⅲ)—Unusual Diene lsomerization in a Diels-Alder reaction241

34.Studies on the total synthesis of Hainanolide(Ⅳ)-Revising the stereochemistry of C2a-H and Introducing the two hydroxy Groups at C3β,C4α positions243

35.Chemical Studies on Decahydroacenaphthylene Compouds-Studies on the Synthesis of Hainanolide--Constuction of Tricycle Intermediate245

36.Study on the total Synthesis of Hainanolide(Ⅴ),Oxidation of the Tricyclic Alkenes with Singlet Oxygen247

三．天然产物的合成249

1.Terpenoids,XI.lnvestigation of nine cactus species.Isolation of two new triterpenes,stellatogenin and machaeric acid249

2.Terpenoids,XVⅡ.The cactus triterpenes thurberogenin and stellatogenin253

3.The constitution of the alloyohimbanes260

4.The neutral constituents of the cactus Lophocereus Shoiiii265

5.The stereochemistry of Reserpine,Deserpidine and related alkaloids274

6.A dihydroresorcinol derivative288

7.黄皮叶中黄皮酰胺的分离和结构测定291

8.Studies on the chemical constituents of Clausena Lansium(Lour)Skeels Ⅱ299

9.黄皮叶化学成分的研究Ⅱ.两个新的环酰胺化合物的结构305

10.Three novel cyclic amides from Clausena Lansium310

11.Asymmctric synthesis of (-)-dehydroclausenamide316

12.Studies on the chemical constituents of Clausena Lansium(Lour)Skeels Ⅲ，The structural elucidation of homo-and Zeta-clausenamide324

13.Studies on the chemical constituents of clausena Lansium(Lour.)Skeels Ⅳ,The structural elucidation of seco and secodemethyl clausenamide326

14.Preliminary studies on the kinetic resolution of methyl erythro-phenylglycerate and methyl t-epoxycinnamate by PLE328

15.去甲原黄皮酰胺苏式异构体的最短合成路线330

16.缩丙酮-（R）-甘油醛加成物的缩酮交换332

17.Study on the intramolecular cyclization through opening of epoxide I Cyclization of N-methyl-N-benzoyl methylene-β-phenyl-α，β-epoxypropionamide in aprotic solvent334

18.Study on the intramolecular cyclization through opening of epoxideⅡ Ring closure of N-methyl-N-benzoyl-methylene-β-phenyl-α，β-epoxypropionamide in protic solvent336

19.Asymmetric syntheses of stereoisomers of secodemethylclausenamide338

20.Total synthesis of clausenamide340

21.Synthesis of stereoisomers of secoclausenamide I and secodemethylclausenamideⅡ342

22.Total synthesis of neoclausenamide and its epimer344

23.黄皮酰胺的合成346

24.An attempt to synthesize homo-clause-namide and zeta-clausenamide.Study of the intramolecular cyclization350

25.Study of Intramolecular Cyclization of N-styryl-oxo-cinnamidesⅡ353

26.国产罗芙木成分的研究 I355

27.鸦胆子甙的化学结构研究359

28.氯霉素类似物——1-对硝基苯-2-（N甲基，二氯乙酰氨基）丙醇-1363

29.仙鹤草根芽中驱绦虫成分——鹤草酚的结构研究（简报）366

30.鹤草酚的结构研究368

31.Quinolone alkaloids from Evodia Rutaecarpa Bentham378

32.吴茱萸化学成分的研究380

33.Quinolone alkaloids from Evodia Rutaecarpa385

34.Studies on the Chemical Constituents of Evodia Rutaecarpa[Juss]Benth389

35.2-烷基取代喹诺酮的合成及生物活性394

36.2-烯基-4（1H）-喹诺酮的合成及生物活性研究401

37.毛莨甙全合成的研究407

四．抗孕药、甾类化合物和棉酚的研究414

1.甾体同化激素的研究414

2.龙舌兰属植物中甾族皂甙元的研究Ⅱ.番麻中甾族皂甙元的分离和鉴定415

3.龙舌兰属植物中甾族皂甙元的研究Ⅱ.剑麻中甾族皂甙元的分离和鉴定428

4.龙舌兰属植物中甾族皂甙元的研究Ⅲ.几种国产龙舌兰麻中甾族皂甙元的分离和鉴定445

5.环失碳19-去甲基双炔甾族化合物的合成452

6.长效避孕药— — 17β—甾醇酯的合成459

7.18-甲基炔诺酮中间体的拆分464

8.17β-甾醇酯肟-3的合成及其异构体分离鉴定468

9.由消旋棉酚拆分得（-）棉酚471

10.Resolution of Racemic gossypol472

11.消旋棉酚拆分的研究I.（S）-1-甲基苯乙胺缩（±）棉酚六乙酸酯的分离474

12.Resolution of Racemic gossypol480

13.Absolute Configuration of Gossypol488

14.Selective inhibition of human immunodeficiency virus type 1 replication by the (-)but not the (+)enantiomer of gossypol491

15.消旋棉酚拆分的研究Ⅱ.手性α-甲基苯乙胺及α-甲基苯胺为拆分剂494

16.消旋棉酚拆分的研究Ⅲ.胺缩棉酚理化性质的研究500

17.消旋棉酚拆分的研究Ⅳ.苏（-）或（+）-1-（对硝基苯基）-1，3-二羟基丙胺-2为拆分剂507

18.Chiroptical Properties of stereoisomeric conjugated oximes512

19.棉酚及其相关化合物的分子力学和分子图形学研究515

20.Anti-HIV-l activity and cellular pharmacology of various analogs of gossypol518

五、专利523

六、专著525

七、附录526

1.按年序排列的论文目录（包括作者、论文题目、杂志、发表时间）527

2.获奖研究项目534

3.培养的研究生535